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建立了ICP-MS测定纺织品中4种有机锡化合物的快速有效检测方法。样品经提取后,在最佳仪器条件下筛查纺织品中有机锡化合物。结果显示:该法具有良好线性(r~2>0.999);方法的检出限<2.0μg/kg;加标回收率在72.9%~87.8%;相对标准偏差在7.63%以内。可见,该方法准确、可靠,适用于快速筛查生态纺织品中4种有机锡化合物的日常检测。
A rapid and effective method for the determination of four organotin compounds in textiles by ICP-MS was established. After the sample is extracted, the organotin compounds in the textile are screened under the best instrument conditions. The results showed that the method showed a good linearity (r ~ 2> 0.999). The detection limit of the method was less than 2.0μg / kg. The recoveries were in the range of 72.9% ~ 87.8%. The relative standard deviations were within 7.63%. Visible, the method is accurate and reliable, suitable for rapid screening of eco-textiles in the four kinds of organic tin compounds routine testing.